Obtaining Ca(H2Po4)(2)·H2O, Monocalcium Phosphate Monohydrate, Via Monetite From Brushite By Using Sonication

Laboratory of Materials and Environmental Sciences, Faculty of Sciences of Sfax, Soukra Road km 4—B. P. no 802−3038, Sfax, Tunisia
Publication History Received12 June 2015Accepted2 August 2015Revised24 July 2015Published online11 August 2015Published inissue 26 August 2015

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Monocalcium phosphate monohydrate (MCPM) was obtained by water extraction of triple superphosphate. The solubility of MCPM is 783.1 g/L, and is entirely soluble. Saturated MCPM solution dissociates into free phosphoric acid and monetite (CaHPO4), but evaporation to dryness by spray drying forms MCPM during crystallization. Complete characterization by infrared, X-ray diffraction, and scanning electron microscopies and NMR is reported for MCPM and the derived pyrophosphates.

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